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ChemicalBook CAS DataBase List 3-bromo-1H-indazole-7-carbonitrile
945762-00-5

3-bromo-1H-indazole-7-carbonitrile synthesis

5synthesis methods
1H-INDAZOLE-7-CARBONITRILE

256228-64-5
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3-bromo-1H-indazole-7-carbonitrile

945762-00-5
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Yield:945762-00-5 83%

Reaction Conditions:

with NBS in N,N-dimethyl-formamide at 20; for 2 h;

Steps:

A.1 Step 1 :

To a solution of 1H-indazole-7-carbonitrile (1.00 g, 6.98 mmol) in N,N- dimethylformamide (10 mL ) was added N-bromosuccinimide (1.24 g, 6.98 mmol) at room temperature. The mixture was stirred at room temperature for 2 h. The mixture was diluted with water. The solids were collected by filtration and dried under vacuum to afford 3-bromo-1 H-indazole-7-carbonitrile (1.30 g, 83%) as a white solid. MS m/z 222.0 [M+1]+.

References:

WO2022/20342,2022,A1 Location in patent:Page/Page column 40; 159