3-AMINOBENZOYLMETHYLAMIDE synthesis
- Product Name:3-AMINOBENZOYLMETHYLAMIDE
- CAS Number:25900-61-2
- Molecular formula:C8H10N2O
- Molecular Weight:150.18
3400-26-8
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$15.00/5mg
25900-61-2
100 suppliers
$16.00/1g
Yield: 100%
Reaction Conditions:
with hydrogen;palladium 10% on activated carbon in methanol at 20;
Steps:
25.2
A mixture of N-methyl-3-nitro-benzamide (2.47 g, 13.71 mmol) and 10% Pd/C (0.5 g) in methanol (50 ML) was hydrogenated at room temperature and atmospheric pressure overnight.The reaction mixture was filtered through a Celite pad and concentrated.The crude material was used in the next step without further purification. (Yield 2.06 g, 100%).
References:
Chen, Jian Jeffrey;Luk, Kin-Chun Thomas US2004/97493, 2004, A1 Location in patent:Page/Page column 24
3400-26-8
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$15.00/5mg
7291-02-3
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$45.00/1g
25900-61-2
100 suppliers
$16.00/1g
121-92-6
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$6.00/25g
25900-61-2
100 suppliers
$16.00/1g