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15945-28-5

3,5-DICHLORO-4-METHOXYBENZOIC ACID ETHYL ESTER synthesis

1synthesis methods
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Yield:15945-28-5 94%

Reaction Conditions:

Stage #1: ethyl 3,5-dichloro-4-hydroxybenzoatewith potassium carbonate in N,N-dimethyl-formamide at 20;Inert atmosphere;
Stage #2: methyl iodide in N,N-dimethyl-formamide at 20;Inert atmosphere;

References:

Grimster, Neil P.;Connelly, Stephen;Baranczak, Aleksandra;Dong, Jiajia;Krasnova, Larissa B.;Sharpless, K. Barry;Powers, Evan T.;Wilson, Ian A.;Kelly, Jeffery W. [Journal of the American Chemical Society,2013,vol. 135,# 15,p. 5656 - 5668] Location in patent:supporting information

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