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22503-17-9

3,5-DIAMINO-TERT-BUTYLBENZENE synthesis

9synthesis methods
3-BROMO-5-(TERT-BUTYL)ANILINE

156264-80-1
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Yield:22503-17-9 84%

Reaction Conditions:

with bis(triphenylphosphine)nickel(II) chloride;lithium hexamethyldisilazane in toluene at 100; for 18 h;Glovebox;Sealed tube;

References:

Martinez, Gabriel Espinosa;Nugent, Joseph W.;Fout, Alison R. [Organometallics,2018,vol. 37,# 18,p. 2941 - 2944] Location in patent:supporting information

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