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ChemicalBook CAS DataBase List 3-(4-TERT-BUTYL-PHENYL)-PROPENAL
84434-23-1

3-(4-TERT-BUTYL-PHENYL)-PROPENAL synthesis

7synthesis methods
-

Yield: 69%

Reaction Conditions:

with tert.-butylhydroperoxide;Ru(2,4,13,15-tetraphenyl-1,5,12,16-tetraaza-tricyclo[14.2.2.06,11]eicosa-4,6(11),7,9,12-pentaene)Cl2 in acetonitrile at 20; for 3 h;Irradiation;Reagent/catalyst;

Steps:

2.4.1 C-H bond activation of methylstyrenes
General procedure: To a solution of Zn(II)/Ru(II) complex (1.25μmol), methylstyrenes (0.5mmol) and TBHP (1.0mmol) in 10mL of acetonitrile was added at room temperature. After the reaction was stirred under visible light for three hours, (monitored the reaction by LC-MS) solvent was distilled under reduced pressure. Purification of crude products by column chromatography with hexane/dichloromethane (9:1, v/v) as eluent to an afforded pure product (Scheme 2).

References:

Gugulothu, Venkanna;Ahemed, Jakeer;Subburu, Mahesh;Yadagiri, Bhongiri;Mittal, Ritu;Prabhakar, Chetti;Pola, Someshwar [Polyhedron,2019,vol. 170,p. 412 - 423]

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