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ChemicalBook CAS DataBase List 3-(4'-METHOXYPHENYL)PROPYL CHLORIDE
59623-12-0

3-(4'-METHOXYPHENYL)PROPYL CHLORIDE synthesis

11synthesis methods
22255-22-7 Synthesis
3,4',5-TRIMETHOXY-TRANS-STILBENE

22255-22-7
205 suppliers
$5.00/50mg

-

Yield:-

Steps:

Multi-step reaction with 4 steps
1.1: O3 / CH2Cl2; methanol / -78 °C
1.2: 73 percent / Ph3P / CH2Cl2; methanol / 0.5 h
2.1: 76 percent / CH2Cl2 / 5 h / Heating
3.1: H2 / 10 percent Pd/C / ethyl acetate / 20 °C
3.2: 76 percent / LiAlH4 / tetrahydrofuran / 5 h / Heating
4.1: 78 percent / CCl4; Ph3P / 8 h / Heating

References:

Fronza, Giovanni;Fuganti, Claudio;Serra, Stefano;Cisero, Marco;Koziet, Joseph [Journal of agricultural and food chemistry,2002,vol. 50,# 10,p. 2748 - 2754]

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