3',4'-DIMETHYL-BIPHENYL-4-YLAMINE synthesis
- Product Name:3',4'-DIMETHYL-BIPHENYL-4-YLAMINE
- CAS Number:188906-52-7
- Molecular formula:C14H15N
- Molecular Weight:197.28
4471-22-1
20 suppliers
$100.00/5g
615-60-1
155 suppliers
$70.00/500mg
188906-52-7
12 suppliers
$1339.80/1G
Yield:188906-52-7 88 %
Reaction Conditions:
Stage #1: Phenyl-trityl-amine;4-chloro-1,2-dimethylbenzenewith tBuXPhos Pd G3;lithium hexamethyldisilazane in toluene at 80;Inert atmosphere;Glovebox;Sealed tube;
Stage #2: with trifluoroacetic acid in dichloromethane at 0 - 20;Inert atmosphere;Glovebox;Sealed tube;
References:
Lichte, Dominik;Pirkl, Nico;Heinrich, Gregor;Dutta, Sayan;Goebel, Jonas F.;Koley, Debasis;Goo?en, Lukas J. [Angewandte Chemie - International Edition,2022,vol. 61,# 47,art. no. E202210009][Angew. Chem.,2022,vol. 134,# 47] Location in patent:supporting information
62-53-3
679 suppliers
$10.00/1g
188906-52-7
12 suppliers
$1339.80/1G