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ChemicalBook CAS DataBase List 3-(4-CHLOROPHENYL)-1H-PYRAZOL-5-AMINE
78583-81-0

3-(4-CHLOROPHENYL)-1H-PYRAZOL-5-AMINE synthesis

8synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 3 steps
1.1: sulfuric acid / ethanol / 12 h / Reflux
2.1: sodium hydride / toluene / 0.5 h / 0 °C
2.2: 12 h / 100 °C
3.1: hydrazine hydrate / ethanol / 12 h / Reflux

References:

NORGINE B.V.;BAKTHAVATCHALAM, Rajagopal;BASU, Manas Kumar;BEHERA, Ajit Kumar;VENKATESHAPPA, Chandregowda;HEWSON, Christopher Alexander;KADNUR, Sanjay Venkatachalapathi;KALINDJIAN, Sarkis Barret;KULKARNI, Bheemashankar;SAXENA, Rohit;SURESH, Juluri;VISWANATHAN, Vellarkad;ZAINUDDIN, Mohd;DHARSHINIS, Akila Parvathy;KRISTAM, Rajenda WO2015/97122, 2015, A1

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