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ChemicalBook CAS DataBase List 3,4,5-Trimethoxybenzyl alcohol
3840-31-1

3,4,5-Trimethoxybenzyl alcohol synthesis

7synthesis methods
-

Yield:3840-31-1 100%

Reaction Conditions:

with sodium tetrahydroborate in methanol at 0 - 20; for 4 h;

Steps:

Typical Procedures for the Preparation of Compounds 6A'- G' and 7A'- H'.
General procedure: To a solution of 3,4-dimethoxybenzaldehyde (1 g, 6 mmol) in methanol was added NaBH4 (0.27, 7.2 mmol) at 0 °C. The reaction mixture was stirred at room temperature for 4 h, quenched with 3% aqueous HCl solution, and evaporated to dryness. The residue was extracted with CH2Cl2 and the organic layer was dried with MgSO4. Evaporation of the dried organic layer yielded 0.96g (3,4-dimethoxyphenyl)methanol (6D0) as a white solid.

References:

Kim, Sung-Soo;Fang, Yuanying;Park, Haeil [Bulletin of the Korean Chemical Society,2015,vol. 36,# 6,p. 1676 - 1680] Location in patent:supporting information

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