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ChemicalBook CAS DataBase List 2-Undecanone
112-12-9

2-Undecanone synthesis

9synthesis methods
Can be isolated from natural oils by fractional distillation; also by dry distillation of calcium acetate and calcium caprylate, or by boiling octylacetoacetic acid ethyl ester with and alcoholic KOH solution.
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Yield:112-12-9 99%

Reaction Conditions:

with sodium bromite;4-benzoxy-2,2,6,6-tetramethylpiperidine-N-oxyl;sodium hydrogencarbonate in dichloromethane;water; for 2 h;Ambient temperature;

References:

Inokuchi, Tsutomo;Matsumoto, Sigeaki;Nishiyama, Tokio;Torii, Sigeru [Journal of Organic Chemistry,1990,vol. 55,# 2,p. 462 - 466]

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