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ChemicalBook CAS DataBase List 2-PHENYL-PYRIMIDINE-5-CARBOXYLIC ACID METHYL ESTER
64074-29-9

2-PHENYL-PYRIMIDINE-5-CARBOXYLIC ACID METHYL ESTER synthesis

2synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 3 steps
1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.75 h / 20 °C / Inert atmosphere
1.2: 0.5 h / 20 °C / Inert atmosphere
2.1: sodium periodate / dichloromethane / 2 h / 22 °C / Inert atmosphere
2.2: Inert atmosphere
3.1: 1,4-dioxane / 0.08 h / 22 °C

References:

Anderson, Erin D.;Boger, Dale L. [Journal of the American Chemical Society,2011,vol. 133,# 31,p. 12285 - 12292]