2-(DI-T-BUTYLPHOSPHINO)-2'-METHYLBIPHENYL synthesis
- Product Name:2-(DI-T-BUTYLPHOSPHINO)-2'-METHYLBIPHENYL
- CAS Number:255837-19-5
- Molecular formula:C21H29P
- Molecular Weight:312.43
16419-60-6
380 suppliers
$9.00/1g
255837-19-5
168 suppliers
$8.00/250mg
Yield:-
Steps:
Multi-step reaction with 2 steps
1.1: bis-triphenylphosphine-palladium(II) chloride; potassium carbonate / 1,2-dimethoxyethane; water / 5 h / 80 °C / Inert atmosphere
2.1: n-butyllithium / diethyl ether; hexane / 2 h / 0 °C / Inert atmosphere
2.2: 1 h / 20 °C / Inert atmosphere
References:
Zhang, Heng;Hu, Rong-Bin;Zhang, Xiao-Yu;Li, Shi-Xia;Yang, Shang-Dong [Chemical Communications,2014,vol. 50,# 36,p. 4686 - 4689]
583-55-1
470 suppliers
$7.00/5g
255837-19-5
168 suppliers
$8.00/250mg