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39065-43-5

2-CYANO-3-PHENYLPYRIDINE synthesis

3synthesis methods
55758-02-6 Synthesis
3-Bromo-2-cyanopyridine

55758-02-6
270 suppliers
$6.00/1g

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Yield:39065-43-5 73 %

Reaction Conditions:

Stage #1: 3-bromopyridine-2-carbonitrile;phenylboronic acidwith potassium carbonate;triphenylphosphine in water;Inert atmosphere;Suzuki-Miyaura Coupling;
Stage #2: with palladium diacetate in 1,2-dimethoxyethane;water;Inert atmosphere;Glovebox;Reflux;

References:

Vaid, Thomas P.;Cook, Monique E.;Scott, Jessica D.;Borjesson Carazo, Marino;Ruchti, Jonathan;Minteer, Shelley D.;Sigman, Matthew S.;McNeil, Anne J.;Sanford, Melanie S. [Chemistry - A European Journal,2022,vol. 28,# 70,art. no. E202202147]

7677-24-9 Synthesis
Trimethylsilyl cyanide

7677-24-9
385 suppliers
$19.00/5g

39065-45-7 Synthesis
5-PHENYLPYRIDINE-2-CARBONITRILE

39065-45-7
42 suppliers
inquiry

36146-27-7 Synthesis
3-Phenylisonicotinonitrile

36146-27-7
6 suppliers
inquiry

1131-48-2 Synthesis
3-PHENYLPYRIDINE-N-OXIDE

1131-48-2
16 suppliers
inquiry

7677-24-9 Synthesis
Trimethylsilyl cyanide

7677-24-9
385 suppliers
$19.00/5g

39065-45-7 Synthesis
5-PHENYLPYRIDINE-2-CARBONITRILE

39065-45-7
42 suppliers
inquiry