2-CHLORO-N-(2,3,4,5,6-PENTAFLUOROPHENYL)ACETAMIDE synthesis
- Product Name:2-CHLORO-N-(2,3,4,5,6-PENTAFLUOROPHENYL)ACETAMIDE
- CAS Number:70426-73-2
- Molecular formula:C8H3ClF5NO
- Molecular Weight:259.56
771-60-8
233 suppliers
$10.00/1g
70426-73-2
20 suppliers
$103.00/1g
Yield:70426-73-2 94%
Steps:
262.A 2-chloro-N-(pentafluorophenyl)acetamide
EXAMPLE 262A 2-chloro-N-(pentafluorophenyl)acetamide The procedure described in Example 22A was followed, substituting pentafluorophenylamine for 3,4,5-trimethoxyaniline to provide the title compound (94% yield) as a tan solid. 1H NMR (300 MHz, DMSO-d6) δ3.31 (s, 2H), 10.48 (br s, 1H); MS (DCI/NH3) m/e 259 (M+H)+; 277 (M+NH4)+.
References:
US2004/29887,2004,A1