2-CHLORO-5-METHOXYBENZONITRILE synthesis

4synthesis methods

Product Name:2-CHLORO-5-METHOXYBENZONITRILE
CAS Number:127667-00-9
Molecular formula:C8H6ClNO
Molecular Weight:167.59

623-12-1 Synthesis

623-12-1
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Yield:-

Steps:

Multi-step reaction with 3 steps
1.1: n-butyllithium / tetrahydrofuran / 2 h / -78 °C
1.2: -78 - 20 °C
2.1: hydroxylamine hydrochloride / ethanol / 4 h / Reflux
3.1: acetic anhydride; triethylamine / tetrahydrofuran

References:

Hunan Huateng Pharmaceutical Co., Ltd.;Bu Gonggaofamingren CN107400099, 2017, A

Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-

1000210-73-0
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127667-00-9
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References

13719-61-4
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References

2401-24-3 Synthesis

2401-24-3
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544-92-3
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References