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ChemicalBook CAS DataBase List 2-Chloro-3-methyl-4-nitropyridine 1-oxide
60323-95-7

2-Chloro-3-methyl-4-nitropyridine 1-oxide synthesis

1synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: 3-chloro-benzenecarboperoxoic acid / chloroform / 18 h / 0 - 20 °C
2: sulfuric acid; sodium nitrate / 18 h / 0 °C

References:

Radix, Sylvie;Hallé, Fran?ois;Mahiout, Zahia;Teissonnière, Amélie;Bouchez, Grégoire;Auberger, Ludovic;Barret, Roland;Lomberget, Thierry [Helvetica Chimica Acta,2022,vol. 105,# 3,art. no. E202100211]

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