2,6-Dimethylterephthalonitrile synthesis

4synthesis methods

Product Name:2,6-Dimethylterephthalonitrile
CAS Number:95216-09-4
Molecular formula:C10H8N2
Molecular Weight:156.1839

1,4-Benzenedicarbonitrile, 2,6-bis(bromomethyl)-

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95216-09-4
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Yield:-

Steps:

Multi-step reaction with 3 steps
1: 40 percent / NaOH / benzene; aq. ethanol; 2-methyl-propan-2-ol / 8 h / Heating
2: 85 percent / 85percent H₂O₂ / CHCl₃; acetic acid / 42 h / 20 °C
3: 6 mg / 480 - 500 °C / 0 - 0.01 Torr

References:

Staab, Heinz A.;Schanne, Lothar;Krieger, Claus;Taglieber, Volker [Chemische Berichte,1985,vol. 118,# 3,p. 1204 - 1229]

3,11-Dithiatricyclo[11.3.1.159]octadeca-1(17),5,7,9(18),13,15-hexaene-7,18-dicarbonitrile, 15,17-dimethoxy-, stereoisomer (9CI)

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References

1,4-Benzenedicarbonitrile, 2,6-dimethyl-, N1-oxide

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95216-09-4
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References

Benzonitrile, 4-formyl-3,5-dimethyl- (9CI)

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References