2,6-Dichlorobenzoxazole synthesis
- Product Name:2,6-Dichlorobenzoxazole
- CAS Number:3621-82-7
- Molecular formula:C7H3Cl2NO
- Molecular Weight:188.01
19932-84-4
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$7.00/1g
3621-82-7
325 suppliers
$22.00/5g
Yield:3621-82-7 95.2%
Reaction Conditions:
with iron(III) chloride;phosphorus pentachloride in toluene at 60; for 0.5 h;Temperature;Reagent/catalyst;
Steps:
1-4 Example 1: A preparation method of high yield 2,6-dichlorobenzoxazole, the operation is as follows
In a 500 ml three-necked flask, 250 ml of toluene was added, 0.1 mol of 6-chlorobenzoxazolone, 25 g of phosphorus pentachloride, 0.5 g of polyphosphoric acid and 0.5 g of ferric chloride were added, and the mixture was heated to 60 °C with stirring. After stirring for 0.5 h,After the post-treatment, the product had a content of 2,6-dichlorobenzoxazole of 98.5% and a yield of 95.2 %
References:
Anhui Feng Le Agrochemical Co., Ltd.;Zhou Kanglun;Su Chaohui;Shi Yimin CN109761928, 2019, A Location in patent:Paragraph 0009; 0016-0023
22876-20-6
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$31.80/1gm:
3621-82-7
325 suppliers
$22.00/5g
59-49-4
329 suppliers
$6.00/5g
3621-82-7
325 suppliers
$22.00/5g
22876-20-6
117 suppliers
$31.80/1gm:
3621-82-7
325 suppliers
$22.00/5g
28443-50-7
234 suppliers
$21.00/5g
3621-82-7
325 suppliers
$22.00/5g