2,5-DIMETHYLPHENYL ISOTHIOCYANATE synthesis
- Product Name:2,5-DIMETHYLPHENYL ISOTHIOCYANATE
- CAS Number:19241-15-7
- Molecular formula:C9H9NS
- Molecular Weight:163.24
75-15-0
248 suppliers
$40.00/100 g
95-78-3
266 suppliers
$10.00/1g
19241-15-7
45 suppliers
$31.00/1 g
Yield:-
Reaction Conditions:
Stage #1:carbon disulfide;2,5-Dimethylaniline with triethylamine for 12 h;Cooling with ice;
Stage #2: with chloroformic acid ethyl ester in chloroform at 25; for 6 h;
References:
Qin, Junhu;Zhu, Mei;Zhu, Hongmei;Zhang, Liqiong;Fu, Yihong;Liu, Jiamin;Wang, Zhenchao;OuYang, Guiping [Phosphorus, Sulfur and Silicon and the Related Elements,2020,vol. 195,# 7,p. 592 - 599]
