2,4-DICHLORO-5-FLUOROBENZYL ALCOHOL synthesis
- Product Name:2,4-DICHLORO-5-FLUOROBENZYL ALCOHOL
- CAS Number:219765-56-7
- Molecular formula:C7H5Cl2FO
- Molecular Weight:195.02
86522-89-6
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219765-56-7
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Yield:-
Steps:
94.1 Preparation Example 94-1 2,4-Dichloro-5-fluorobenzyl alcohol
In the same manner as in Preparation Example 74-4, the objective compound (1.00 g) was obtained as white crystals from 2,4-dichloro-5-fluorobenzoic acid (1.25 g). 1H-NMR(CDCl3): 1.96(1H, t, J=7 Hz), 4.73(2H, d, J=7 Hz), 7.35(1H, d, J=9 Hz), 7.40(1H, d, J=7 Hz).
References:
Fujisawa Pharmaceutical Co., Ltd. US6348474, 2002, B1 Location in patent:Page column 128