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ChemicalBook CAS DataBase List 2-(4-Aminophenyl)ethylamine
13472-00-9

2-(4-Aminophenyl)ethylamine synthesis

13synthesis methods
24954-67-4 Synthesis
4-NITRO-PHENETHYLAMINE

24954-67-4
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Yield:13472-00-9 100%

Reaction Conditions:

with hydrogen in methanol at 20; under 760.051 Torr;

Steps:

20.1 Step 1. 4-(2-aminoethyl)aniline
2-(4-Nitrophenypethanamine (5.0 g, 30 mmol) and Raney Ni (500 mg) were added to methanol (50 mL) and the mixture was stirred under 1 atmosphere of hydrogen overnight. The reaction mixture was filtered, Raney Ni was washed with methanol (50 mL×4), and the filtrate was dried by rotary evaporation to give 4-(2-aminoethyl)aniline (4.1 g, 30 mmol), yield: 100%.

References:

Shanghai Zhimeng Biophama Co., Ltd.;CHEN, Huanming US2019/152963, 2019, A1 Location in patent:Paragraph 0342-0344

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