2,4,6-TRI-TERT-BUTYL-N-(TRIMETHYLSILYL)ANILINE synthesis
1synthesis methods
- Product Name:2,4,6-TRI-TERT-BUTYL-N-(TRIMETHYLSILYL)ANILINE
- CAS Number:101455-63-4
- Molecular formula:C21H39NSi
- Molecular Weight:333.63
Yield:101455-63-4 94.3%
Reaction Conditions:
Stage #1: 2,4,6-Tri-tert-butylanilinewith n-butyllithium in tetrahydrofuran at 20; for 0.5 h;Inert atmosphere;
Stage #2: chloro-trimethyl-silane in tetrahydrofuran at 0; for 12 h;Inert atmosphere;
References:
Bresien, Jonas;Schulz, Axel;Thomas, Max;Villinger, Alexander [European Journal of Inorganic Chemistry,2019,vol. 2019,# 9,p. 1279 - 1287] Location in patent:supporting information