2,3-DINITROANILINE synthesis
- Product Name:2,3-DINITROANILINE
- CAS Number:602-03-9
- Molecular formula:C6H5N3O4
- Molecular Weight:183.12
60956-27-6
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602-03-9
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Yield:602-03-9 93%
Reaction Conditions:
with sodium methylate in methanol; for 3 h;Reflux;
Steps:
A.B B.
B. 2,3-dinitroaniline To a solution of N-(2,3-dinitrophenyl)acetamide (3.0 g) in methanol (200 mL) was added sodium methoxide (72 mg). The stirred solution was heated at reflux for 3 hours. Water was added to the solution (300 mL) and the yellow solid precipitate was collected and dried to give the desired product (2.27 g, 93%). Chemical Formula: C6H5N3O4 Molecular Weight: 183.12; MS (ES) m/z 184
References:
US2010/120779,2010,A1 Location in patent:Page/Page column 16
122-28-1
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602-03-9
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95182-27-7
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602-03-9
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602-03-9
33 suppliers
$440.00/1g