天堂网亚洲,天天操天天搞,91视频高清,菠萝蜜视频在线观看入口,美女视频性感美女视频,95丝袜美女视频国产,超高清美女视频图片

Welcome to chemicalbook!
Chinese English Japanese Germany Korea
400-158-6606
Try our best to find the right business for you.
Do not miss inquiry messages Please log in to view all inquiry messages.

Welcome back!

ChemicalBook CAS DataBase List 2,3,4,5,6-PENTAFLUOROPHENYLACETONITRILE
653-30-5

2,3,4,5,6-PENTAFLUOROPHENYLACETONITRILE synthesis

13synthesis methods
-

Yield: 97%

Reaction Conditions:

with sulfuric acid;acetic acid in water at 20; for 16.5 h;Reflux;

Steps:

2.2
Step2: Add in the reactorIntermediate A-2-1 (2.79 g, 10 mmol),50% acetic acid (4.10 mL) and sulfuric acid (0.2 mL),Stir after 16 hours of reflux,After the mixture is cooled to room temperature,The reaction was terminated by dropwise addition of 10 mL of cold distilled water.After stirring for 0.5 h,The reaction mixture was extracted with distilled water and chloroform.It was then concentrated to give intermediate A-2-2 (1.95 g, 97%).

References:

Changchun Hai Purunsi Technology Co., Ltd.;Dong Xiuqin;Cai Hui CN109134311, 2019, A Location in patent:Paragraph 0090; 0091; 0093

2,3,4,5,6-PENTAFLUOROPHENYLACETONITRILE Related Search: