2-(2-phenylethynyl)pyridine synthesis
13synthesis methods
- Product Name:2-(2-phenylethynyl)pyridine
- CAS Number:13141-42-9
- Molecular formula:C13H9N
- Molecular Weight:179.22
Yield:13141-42-9 100%
Reaction Conditions:
with pyrrolidine;bis(η3-allyl-μ-chloropalladium(II));triphenylphosphine;1-butyl-3-methylimidazolium Tetrafluoroborate at 100; for 4 h;Inert atmosphere;Heck alkynylation;
References:
Saleh, Samer;Picquet, Michel;Meunier, Philippe;Hierso, Jean-Cyrille [Tetrahedron,2009,vol. 65,# 34,p. 7146 - 7150] Location in patent:experimental part