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886578-15-0

1H-INDOLE-3-SULFONYL CHLORIDE synthesis

2synthesis methods
1H-Indole-3-sulfonic acid, compd. with pyridine (1:1)

40801-88-5
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1H-INDOLE-3-SULFONYL CHLORIDE

886578-15-0
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Yield:886578-15-0 2.64 g

Reaction Conditions:

with trichlorophosphate in sulfolane;acetonitrile at 0 - 70; for 1 h;Inert atmosphere;

References:

Schneider, Cedric;Broda, Ellen;Snieckus, Victor [Organic Letters,2011,vol. 13,# 14,p. 3588 - 3591] Location in patent:supporting information; experimental part

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