[S-(R*,R*)]-1,3,4,5-Tetrahydro-3-[(1-phenylethyl)amino]-2H-1-benzazepin-2-one synthesis
- Product Name:[S-(R*,R*)]-1,3,4,5-Tetrahydro-3-[(1-phenylethyl)amino]-2H-1-benzazepin-2-one
- CAS Number:197658-50-7
- Molecular formula:C18H20N2O
- Molecular Weight:280.36
![3-Bromo-1,3,4,5-tetrahydro-2H-benzo[b]azepin-2-one](/CAS/GIF/86499-96-9.gif)
86499-96-9
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Yield:-
Steps:
Multi-step reaction with 2 steps
1: 93 percent / Na2CO3, propylene glycol / 3.5 h / 130 °C
2: 88 percent / odorless mineral spirits / 16 h / 140 °C
References:
Shieh;Carlson;Zaunius [Journal of Organic Chemistry,1997,vol. 62,# 23,p. 8271 - 8272]
![2H-1-Benzazepin-2-one, 1,3,4,5-tetrahydro-3-[[(1S)-1-phenylethyl]amino]-](/CAS/20210305/GIF/197658-51-8.gif)
197658-51-8
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197658-50-7
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