4'-ACETAMIDO-2'-CARBOXY-4-DIMETHYLAMINO-2-HYDROXYBENZOPHENONE synthesis
- Product Name:4'-ACETAMIDO-2'-CARBOXY-4-DIMETHYLAMINO-2-HYDROXYBENZOPHENONE
- CAS Number:166442-36-0
- Molecular formula:C18H18N2O5
- Molecular Weight:342.35
5466-84-2
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166442-36-0
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Yield:-
Steps:
Multi-step reaction with 3 steps
1: 2.) conc. H2SO4 / 1) toluene, reflux, 6 h; 2) reflux, 8 h
2: H2 / Pd/C / acetic acid / 5 h / Ambient temperature
3: 1.) pyridine, 2.) aq. NaOH / 1) room temperature, 16 h; 2) methanol, reflux, 1 h
References:
Corrie, John E. T.;Craik, James S. [Journal of the Chemical Society. Perkin transactions I,1994,# 20,p. 2967 - 2974]
159435-03-7
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166442-36-0
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108-24-7
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1027597-25-6
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166442-36-0
13 suppliers
$100.00/5mg