1,3-DIETHYL-2-OXO-2,3-DIHYDRO-1H-BENZOIMIDAZOLE-5-CARBALDEHYDE synthesis
- Product Name:1,3-DIETHYL-2-OXO-2,3-DIHYDRO-1H-BENZOIMIDAZOLE-5-CARBALDEHYDE
- CAS Number:14624-85-2
- Molecular formula:C12H14N2O2
- Molecular Weight:218.25
23814-14-4
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$119.00/250mg
14624-85-2
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$485.00/1g
Yield:-
Steps:
Multi-step reaction with 3 steps
1: 50 percent / NaH / dimethylformamide
2: 79 percent / LiBH4 / methanol; tetrahydrofuran / 18 h / Heating
3: 42 percent / TEMPO; NCS; Bu4NCl / CH2Cl2 / 5.5 h / pH 8.6
References:
Dombroski, Mark A.;Letavic, Michael A.;McClure, Kim F.;Barberia, John T.;Carty, Thomas J.;Cortina, Santo R.;Csiki, Csilla;Dipesa, Alan J.;Elliott, Nancy C.;Gabel, Christopher A.;Jordan, Crystal K.;Labasi, Jeff M.;Martin, William H.;Peese, Kevin M.;Stock, Ingrid A.;Svensson, Linne;Sweeney, Francis J.;Yu, Chul H. [Bioorganic and Medicinal Chemistry Letters,2004,vol. 14,# 4,p. 919 - 923]
619-05-6
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14624-85-2
9 suppliers
$485.00/1g
680188-97-0
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14624-85-2
9 suppliers
$485.00/1g