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ChemicalBook CAS DataBase List 4-METHOXYPHENYL 3,6-DI-O-BENZYL-2-DEOXY-2-PHTHALIMIDO-BETA-D-GLUCOPYRANOSIDE
129575-89-9

4-METHOXYPHENYL 3,6-DI-O-BENZYL-2-DEOXY-2-PHTHALIMIDO-BETA-D-GLUCOPYRANOSIDE synthesis

12synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 4 steps
1: p-TsOH*H2O / dimethylformamide / 20 h / 20 °C
2: 61 percent / NaH / dimethylformamide / 20 h / 20 °C
3: 77 percent / p-TsOH*H2O / methanol; dioxane / 1) 1 h, 60 deg C, 2) 45 min, 85 deg C

References:

Nakano;Ito;Ogawa [Carbohydrate Research,1993,vol. 243,# 1,p. 43 - 69]

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