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121190-46-3

1,2-BENZENEDICARBONITRILE, 4-(2,2,3,3-TETRAFLUOROPROPOXY) synthesis

1synthesis methods
31643-49-9 Synthesis
4-Nitrophthalonitrile

31643-49-9
452 suppliers
$6.00/5g

1,2-BENZENEDICARBONITRILE, 4-(2,2,3,3-TETRAFLUOROPROPOXY)

121190-46-3
14 suppliers
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Yield:121190-46-3 50%

Reaction Conditions:

Stage #1: 2,2,3,3-tetrafluoropropanol;4-Nitrophthalonitrile in dimethyl sulfoxide; for 0.166667 h;Inert atmosphere;
Stage #2: with potassium carbonate in dimethyl sulfoxide at 20;Inert atmosphere;

References:

Guerol, Ilke;Durmus, Mahmut;Ahsen, Vefa [European Journal of Inorganic Chemistry,2010,# 8,p. 1220 - 1230] Location in patent:experimental part

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