10-bromobenzo[h]quinoline synthesis

3synthesis methods

Product Name:10-bromobenzo[h]quinoline
CAS Number:152583-10-3
Molecular formula:C13H8BrN
Molecular Weight:258.11

Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-

1000210-73-0
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152583-10-3
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Yield:-

Steps:

Multi-step reaction with 2 steps
1: tetrahydrofuran / 1 h / -35 °C / Inert atmosphere; Schlenk technique; Glovebox
2: ferrocenium(III) tetrafluoroborate; platinum; tetraethylammonium chloride / acetonitrile / 20 °C / Inert atmosphere; Schlenk technique; Glovebox; Electrochemical reaction

References:

Dudkina, Yulia B.;Fayzullin, Robert R.;Lyssenko, Konstantin A.;Gubaidullin, Aidar T.;Kholin, Kirill V.;Levitskaya, Alina I.;Balakina, Marina Yu.;Budnikova, Yulia H. [Organometallics,2019,vol. 38,# 6,p. 1254 - 1263]

230-27-3 Synthesis

230-27-3
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152583-10-3
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References

186268-24-6
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152583-10-3
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References