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ChemicalBook CAS DataBase List 1-PHENYL-3-(TRIMETHYLSILYL)-2-PROPYN-1-&
89530-34-7

1-PHENYL-3-(TRIMETHYLSILYL)-2-PROPYN-1-& synthesis

9synthesis methods
-

Yield:89530-34-7 100%

Reaction Conditions:

Stage #1: trimethylsilylacetylenewith n-butyllithium in tetrahydrofuran at 0; for 1 h;
Stage #2: benzaldehyde in tetrahydrofuran at 0; for 1 h;

References:

Yamabe, Hokuto;Mizuno, Akio;Kusama, Hiroyuki;Iwasawa, Nobuharu [Journal of the American Chemical Society,2005,vol. 127,# 10,p. 3248 - 3249]

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