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ChemicalBook CAS DataBase List 1-NITROBUTANE
627-05-4

1-NITROBUTANE synthesis

11synthesis methods
-

Yield:627-05-4 90%

Steps:

VII EXAMPLE VII
EXAMPLE VII The procedure of Example VI was repeated except 11.0 grams (0.1 mole) of 4-octene was employed as starting material and 27.0 grams of solids composed of calcium nitrate and the calcium salt of the nitroketone were separated by filtration. Extraction and acidification provided 8.7 grams of nitrobutane (92 percent yield) and 7.9 grams of butanoic acid (90 percent yield).

References:

Texaco Inc. US4013697, 1977, A

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