1-METHOXYPYRENE synthesis
- Product Name:1-METHOXYPYRENE
- CAS Number:34246-96-3
- Molecular formula:C17H12O
- Molecular Weight:232.28
1714-29-0
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$6.00/1g
124-41-4
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$12.00/25g
34246-96-3
101 suppliers
$70.00/1g
Yield: 95.2%
Reaction Conditions:
in methanol for 15 h;Inert atmosphere;Reflux;Large scale;
Steps:
2 Example 2:
Under nitrogen protection conditions,Reaction kettle was added 30% sodium methoxide methanol solution 340kg,Warmed to reflux,In three batches were added 1-bromopyrene 170kg,Add a batch every 1 hour,After the reaction was completed 12 hours,Methanol recovery under reduced pressure,Cooled to 40-45 ,Add ice water to stir,Centrifuge,Drying under reduced pressure gave 134.3 kg, yield 95.2%.
References:
Jiangsu Jinghua Tiancheng New Materials Technology Co., Ltd.;Gu Huan;Xu Lili CN106187709, 2016, A Location in patent:Paragraph 0019
67-56-1
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1714-29-0
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34246-96-3
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$70.00/1g
5315-79-7
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77-78-1
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34246-96-3
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$70.00/1g
5315-79-7
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74-88-4
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34246-96-3
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$70.00/1g
129-00-0
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34246-96-3
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$70.00/1g