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ChemicalBook CAS DataBase List 1-Bromo-9-(tert-butyldimethylsilyloxy)nonane
149051-24-1

1-Bromo-9-(tert-butyldimethylsilyloxy)nonane synthesis

4synthesis methods
55362-80-6 Synthesis
9-Bromo-1-nonanol

55362-80-6
285 suppliers
$10.00/1g

18162-48-6 Synthesis
tert-Butyldimethylsilyl chloride

18162-48-6
671 suppliers
$9.00/5g

1-Bromo-9-(tert-butyldimethylsilyloxy)nonane

149051-24-1
19 suppliers
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Yield:149051-24-1 100%

Reaction Conditions:

with 1H-imidazole;dmap in dichloromethane at 0 - 20; for 4 h;Inert atmosphere;

References:

Bailey, Adrian M.;Wolfrum, Susanne;Carreira, Erick M. [Angewandte Chemie - International Edition,2016,vol. 55,# 2,p. 639 - 643][Angew. Chem.,2016,vol. 128,# 2,p. 649 - 653,5] Location in patent:supporting information