1-(3-NITROPHENYLSULFONYL)PIPERIDINE synthesis
- Product Name:1-(3-NITROPHENYLSULFONYL)PIPERIDINE
- CAS Number:91619-31-7
- Molecular formula:C11H14N2O4S
- Molecular Weight:270.3
110-89-4
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$15.96/100ML
84752-61-4
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$46.00/5g
91619-31-7
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$77.00/1g
Yield:91619-31-7 84%
Reaction Conditions:
Stage #1: pyridinium paratoluene sulfonic acidwith trifluoromethanesulfonic acid anhydride;Triphenylphosphine oxide in dichloromethane;
Stage #2: piperidinewith triethylamine in dichloromethane at 0 - 20;
References:
Caddick, Stephen;Wilden, Jonathan D.;Judd, Duncan B. [Journal of the American Chemical Society,2004,vol. 126,# 4,p. 1024 - 1025]