1-(2,4-DICHLORO-PHENYL)-ETHYLAMINE synthesis
- Product Name:1-(2,4-DICHLORO-PHENYL)-ETHYLAMINE
- CAS Number:89981-75-9
- Molecular formula:C8H9Cl2N
- Molecular Weight:190.07
35588-60-4
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Yield:-
Steps:
22 EXAMPLE 22
Content of the oil 1-(2',4'-dichlorophenyl)ethylamine; 91%, 1-(4'-chlorophenyl)ethylamine 2.9%, N-1-(2',4'-dichlorophenyl)ethyl-α-(2',4'-dichlorophenyl)ethylamine; 1.1%, N-acetyl-α-(2',4'-dichlorophenyl)ethylamide; 1.5%, an alcohol obtained by reduction of carbonyl group; not detected. 58.5 g of 1-(2',4'-dichlorophenyl)ethylamine was obtained by distillation; the purity: 99%, boiling point: 130°-132° C./20 mmHg.
References:
Sumitomo Chemical Company, Limited US5739401, 1998, A