1-(2,4,6-Trichlorophenyl)-3-amino-pyrazolin-5-one synthesis

4synthesis methods

Product Name:1-(2,4,6-Trichlorophenyl)-3-amino-pyrazolin-5-one
CAS Number:27241-31-2
Molecular formula:C9H6Cl3N3O
Molecular Weight:278.52

Acetamide, 2-cyano-N-(2,4,6-trichlorophenyl)-

24522-44-9
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1-(2,4,6-Trichlorophenyl)-3-amino-pyrazolin-5-one

27241-31-2
69 suppliers
$85.00/250 mg

Yield:-

Steps:

Multi-step reaction with 4 steps
1: acetic acid / 2 h / Ambient temperature
2: 95 percent / acetic acid / 1.5 h / Heating
3: 58 percent / KOH / ethanol / 10 h / Heating
4: 79 percent / anhydrous hydrogen chloride / ethanol / 1.5 h / Heating

References:

Kim, Chang-Kyu;Zielinski, Paul A.;Maggiulli, Cataldo A. [Journal of Organic Chemistry,1984,vol. 49,# 26,p. 5247 - 5250]

52472-98-7 Synthesis

3-Propeneamido-1-(2,4,6-trichlorophenyl)-5-pyrazolone

52472-98-7
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27241-31-2
69 suppliers
$85.00/250 mg

References

1,2,4-Oxadiazole-3-acetamide, 5-methyl-N-(2,4,6-trichlorophenyl)-

84104-39-2
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27241-31-2
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$85.00/250 mg

References

Propanamide, 3-[(acetyloxy)amino]-3-imino-N-(2,4,6-trichlorophenyl)-

799823-29-3
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27241-31-2
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$85.00/250 mg

References

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