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821-25-0

1,1-dichloroheptane synthesis

10synthesis methods
-

Yield:821-25-0 83%

Steps:

8 Synthesis of 4-Acetamido-2,6-dimethylanisole (7)

Removing the solvent and recrystallizing the resulting solid from hexane-methylene chloride yielded 4-acetamido-2,6-dimethylanisole (7, 5.3 g, 83% yield). Spectral data: 1 H NMR: δ 2.1 (s, 3H), 2.2 (s, 6H), 3.65 (s, 3H), 7.10 (s, 2H), 8.10 (s, 1H); 13 C NMR: δ 16.1, 24.2, 60.0, 121.5, 131.8, 134.3, 154.3, 169.8; CI-HRMS: calcd. for C11 H16 NO2 (M+H+) 194.1181, fnd. 194.1181.

References:

US5674876,1997,A