四乙基鍺(597-63-7)質(zhì)譜(MS)

產(chǎn)品名稱:四乙基鍺

CAS:597-63-7

分子式:C8H20Ge

分子量: 188.88

InChI:InChI=1S/C8H20Ge/c1-5-9(6-2,7-3)8-4/h5-8H2,1-4H3

InChIKey: QQXSEZVCKAEYQJ-UHFFFAOYSA-N

Smiles:[Ge](CC)(CC)(CC)CC

¹HNMR

¹³CNMR

IR1

Mass

MS-NW-8638          
tetraethylgermane
C8H20Ge             (Mass of molecular ion:    190)

   Source Temperature: 260 °C
   Sample Temperature: 130 °C
   Reservoir, 75 eV

      26.0       1.0
      27.0       5.0
      28.0       1.7
      29.0       3.7
      70.0       3.8
      71.0       7.4
      72.0       5.1
      73.0      15.3
      74.0       9.4
      75.0      18.6
      76.0       3.3
      77.0      10.6
      79.0       1.7
      85.0       1.7
      87.0       2.9
      88.0       1.5
      89.0       3.8
      91.0       1.6
      97.0       2.2
      99.0      12.6
     100.0       2.8
     101.0      43.2
     102.0       7.2
     103.0      54.3
     104.0      13.8
     105.0      51.4
     106.0       1.7
     107.0      10.1
     128.0       1.3
     129.0      57.4
     130.0       4.6
     131.0      76.9
     132.0      26.9
     133.0     100.0
     134.0       5.0
     135.0      21.0
     157.0      39.4
     158.0       2.8
     159.0      52.0
     160.0      18.3
     161.0      69.5
     162.0       4.6
     163.0      14.5
     164.0       1.0
     188.0       1.1
     190.0       1.5
     207.0       1.4

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₈ H₂₀ Ge	0.05 ml : 0.5 ml CDCl₃
tetraethylgermane

    Assign.     Shift(ppm)

      A             1.013
      B             0.710

     Hz     ppm     Int.

    430.42   1.077     24
    413.57   1.035    508
    413.09   1.034    621
    405.40   1.015    920
    404.79   1.013   1000
    397.09   0.994    674
    396.61   0.993    556
    294.92   0.738    314
    294.19   0.737    316
    286.99   0.719    712
    286.13   0.716    479
    278.93   0.698    617
    271.12   0.679    213
    270.39   0.677    228

in CDCl3