氯二甲基辛硅烷(18162-84-0)核磁圖(¹³CNMR)

產(chǎn)品名稱:氯二甲基辛硅烷

CAS:18162-84-0

分子式:C10H23ClSi

分子量: 206.83

InChI:InChI=1S/C10H23ClSi/c1-4-5-6-7-8-9-10-12(2,3)11/h4-10H2,1-3H3

InChIKey: DBKNGKYVNBJWHL-UHFFFAOYSA-N

Smiles:[Si](Cl)(C)(C)CCCCCCCC

Mass

MS-NW-8605          
chlorodimethyloctylsilane
C10H23ClSi          (Mass of molecular ion:    206)

   Source Temperature: 250 °C
   Sample Temperature: 140 °C
   Reservoir, 75 eV

      27.0       2.0
      29.0       2.9
      39.0       1.5
      41.0       5.1
      42.0       1.4
      43.0       5.1
      55.0       2.4
      56.0       1.5
      57.0       5.3
      59.0       3.2
      63.0       2.9
      65.0       4.6
      67.0       1.3
      69.0       2.7
      70.0       1.8
      71.0       1.4
      73.0       1.0
      78.0       1.4
      79.0       8.7
      80.0       1.0
      81.0       3.1
      83.0       1.5
      84.0       1.0
      91.0       1.3
      92.0       1.7
      93.0     100.0
      94.0       7.9
      95.0      36.0
      96.0       2.5
      97.0       2.1
     105.0       1.5
     107.0       5.0
     109.0       1.6
     111.0       3.7
     112.0       4.9
     119.0       4.9
     121.0      15.9
     122.0       1.5
     123.0       5.4
     133.0      12.2
     134.0       1.8
     135.0       3.6
     137.0       1.1
     147.0       3.5
     149.0       2.3
     191.0      18.7
     192.0       2.8
     193.0       6.8
     194.0       1.0
     245.0       2.8

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₀ H₂₃ Cl Si	0.05 ml : 0.5 ml CDCl₃
chlorodimethyloctylsilane

    Assign.     Shift(ppm)

      A             1.30
      B             1.27
      C             0.883
      D             0.499
      E             0.028

     Hz     ppm     Int.

    529.05   1.324     60
    519.41   1.300    160
    516.85   1.294    166
    514.28   1.287    192
    506.96   1.269    353
    359.86   0.901    102
    353.15   0.884    296
    346.07   0.866    124
    207.03   0.519     42
    199.22   0.499     66
    191.53   0.480     43
     14.65   0.037     99
     11.35   0.029   1000
      8.06   0.021    105
      3.30   0.009     21

in CDCl3