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CAS No. : | 99-03-6 | MDL No. : | MFCD00007796 |
Formula : | C8H9NO | Boiling Point : | - |
Linear Structure Formula : | CH3C(O)C6H4NH2 | InChI Key : | CKQHAYFOPRIUOM-UHFFFAOYSA-N |
M.W : | 135.16 | Pubchem ID : | 7417 |
Synonyms : |
|
Chemical Name : | 1-(3-Aminophenyl)ethanone |
Signal Word: | Warning | Class: | N/A |
Precautionary Statements: | P280-P305+P351+P338 | UN#: | N/A |
Hazard Statements: | H302 | Packing Group: | N/A |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
35% | With potassium hydroxide; In ethanol; at 5℃; | General procedure: A mixture of 4-hydroxy-3-methoxybenzaldehyde (1.5 g, 10.0 mmol) and 3’-aminoacetophenone (1.4 g, 10.0 mmol) is dissolved in 15 mL of ethanol and allowed to stir for several min at 5 C (ice bath). 10 mL of a40 % KOH solution in water is added dropwise to the flask over several min. The mixture is then allowed to stir at room temperature for approximately 10h. After the reaction was completed, the reaction mixture was neutralized with adilute HCl. The solution was extracted with anhydrous ether(3 × 10 mL). The organic layer was concentrated and purified bysilica gel column chromatography (CH2Cl2/methanol = 94/6). Yield 35 %; |
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