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[ CAS No. 98648-23-8 ] {[proInfo.proName]}

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Chemical Structure| 98648-23-8
Chemical Structure| 98648-23-8
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Product Details of [ 98648-23-8 ]

CAS No. :98648-23-8 MDL No. :MFCD06200931
Formula : C13H9NO3 Boiling Point : -
Linear Structure Formula :- InChI Key :MGHIIGWDUVNPPV-UHFFFAOYSA-N
M.W : 227.22 Pubchem ID :2763586
Synonyms :

Safety of [ 98648-23-8 ]

Signal Word:Warning Class:N/A
Precautionary Statements:P280-P305+P351+P338 UN#:N/A
Hazard Statements:H302 Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 98648-23-8 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 98648-23-8 ]

[ 98648-23-8 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 586-78-7 ]
  • [ 128376-65-8 ]
  • [ 98648-23-8 ]
  • 2
  • [ 15862-94-9 ]
  • [ 98648-23-8 ]
  • 2-(4,5-dimethoxy-2-nitrophenyl)-1-(4'-nitro[1,1'-biphenyl]-4-yl)ethanol [ No CAS ]
YieldReaction ConditionsOperation in experiment
51% General procedure: To a glass vessel capable of being sealed with Teflon cap (for microwave vials) were added 1 and benzaldehyde derivative (3 equiv.). The vessel was capped and then, evacuated and backfilled with N2 (process repeated 3X). Anhydrous DMF (3.5mL/mmol) was introduced and the solution was vigorously stirred for 20min at-20C. TDAE was added slowly and the mixture was stirred for 1h. Then, the reaction was stirred at room temperature overnight. After LC-MS analysis clearly showed that the chloride had been totally consumed, the reaction was hydrolysed with distilled water. The mixture was then extracted with dichloromethane. The combined organic layers were washed with water and brine, dried over Na2SO4, filtered off and concentrated under reduced pressure to afford the corresponding crude product 3.
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