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[ CAS No. 98-33-9 ] {[proInfo.proName]}

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Cat. No.: {[proInfo.prAm]}
Chemical Structure| 98-33-9
Chemical Structure| 98-33-9
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Product Details of [ 98-33-9 ]

CAS No. :98-33-9 MDL No. :MFCD00025198
Formula : C7H9NO3S Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W : 187.22 Pubchem ID :-
Synonyms :

Safety of [ 98-33-9 ]

Signal Word:Warning Class:N/A
Precautionary Statements:P261-P280-P305+P351+P338 UN#:N/A
Hazard Statements:H317-H319-H412 Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 98-33-9 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 98-33-9 ]

[ 98-33-9 ] Synthesis Path-Downstream   1~4

  • 1
  • [ 98-33-9 ]
  • [ 6291-02-7 ]
  • 2
  • strontium nitrate [ No CAS ]
  • [ 92-70-6 ]
  • [ 98-33-9 ]
  • [ 81-16-3 ]
YieldReaction ConditionsOperation in experiment
With hydrogenchloride; sodium hydroxide; calcium chloride; sodium nitrite; In water; EXAMPLE 1 A solution of 24.2 grams (0.1294 mole) of pure 6-amino-m-toluenesulfonic acid and 1.2 grams (0.0054 mole) of 2-naphthylamine-1-sulfonic acid is prepared in 500 ml of water by adding 57 ml of a 10% solution of sodium hydroxide and adjusting the pH to 11.5. A solution of 35.6 grams of calcium chloride and 1.5 grams of strontium nitrate in 100 ml of water is added thereto and the mixture cooled to 0 C. with ice. The amines are diazotized by adding 35 ml (0.14 mole) of 4 N sodium nitrite, followed by 150 ml (0.411 mole) of 10% hydrochloric acid. The mixture is stirred for about 3 minutes at 0 C., while maintaining excess nitrous acid. 2-Hydroxy-3-naphthoic acid (28.0 grams, 0.1489 mole) is dissolved in 500 ml of water by adding 180 ml of 10% sodium hydroxide.
  • 4
  • [ 98-33-9 ]
  • [ 53848-17-2 ]
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