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[ CAS No. 94-98-4 ] {[proInfo.proName]}

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Cat. No.: {[proInfo.prAm]}
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Chemical Structure| 94-98-4
Chemical Structure| 94-98-4
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Product Details of [ 94-98-4 ]

CAS No. :94-98-4 MDL No. :MFCD00025575
Formula : C9H13N Boiling Point : -
Linear Structure Formula :- InChI Key :GBSUVYGVEQDZPG-UHFFFAOYSA-N
M.W : 135.21 Pubchem ID :66761
Synonyms :

Safety of [ 94-98-4 ]

Signal Word:Danger Class:8
Precautionary Statements:P261-P280-P305+P351+P338-P310 UN#:2735
Hazard Statements:H302-H314 Packing Group:Ⅲ
GHS Pictogram:

Application In Synthesis of [ 94-98-4 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 94-98-4 ]

[ 94-98-4 ] Synthesis Path-Downstream   1~15

  • 1
  • [ 21789-36-6 ]
  • [ 94-98-4 ]
YieldReaction ConditionsOperation in experiment
100% With lithium aluminium tetrahydride; In tetrahydrofuran; diethyl ether; at 0 - 20℃; for 3h; (2,4-Dimethylphenyl)methanamine: Lithium aluminum hydride 1M solution in THF (15.2 ml, 15.2 mmol) was placed in a pre-dried flask under argon at 0 C.; a solution of 2,4-dimethylbenzonitrile (1.0 g, 7.6 mmol) in 15 ml of anhydrous ether was added drop wisely. After the addition, the reaction mixture was warmed up slowly to r.t. and stirred for 3 hr. then it was cooled to 0 C., anhydrous sodium sulfate was added, and 1 ml of water was added drop wisely. The mixture was diluted with ethyl acetate, the insoluble matter was filtered out, the filtrate was washed with water and brine, dried over MgSO4, filtered and evaporated to give 1.03 g of pure (2,4-dimethylphenyl)methanamine in quantitative yield without purification.
With lithium aluminium tetrahydride; In tetrahydrofuran; diethyl ether; at 0 - 20℃; for 3h;Inert atmosphere; Lithium aluminum hydride 1M solution in THF (15.2 ml, 15.2 mmol) was placed in a pre-dried flask under argon at 0 C.; a solution of 2,4-dimethylbenzonitrile (1.0 g, 7.6 mmol) in 15 ml of anhydrous ether was added drop wisely. After the addition, the reaction mixture was warmed up slowly to r.t. and stirred for 3 hr. then it was cooled to 0 C., anhydrous sodium sulfate was added, and 1 ml of water was added drop wisely. The mixture was diluted with ethyl acetate, the insoluble matter was filtered out, the filtrate was washed with water and brine, dried over MgSO4, filtered and evaporated to give 1.03 g of pure (2,4-dimethylphenyl)methanamine in quantitative yield without purification.
  • 2
  • [ 874014-36-5 ]
  • [ 94-98-4 ]
YieldReaction ConditionsOperation in experiment
28% With hydrazine; In ethanol; at 80℃; for 1h; Reference Example 64 2,4-dimethylbenzylamine To a solution (150 mL) of 2-[(2,4-dimethylphenyl)methyl]-1H-isoindole-1,3 (2H)-dione (15.0 g) obtained in Reference Example 62 in ethanol was added hydrazine monohydrate (3.0 g) at 0C. The reaction mixture was stirred at 80C for 1 hr. After cooling to room temperature, water was added to the reaction mixture and the mixture was extracted with ethyl acetate. 1N Hydrochloric acid was added to the obtained organic layer, and the aqueous layer was washed with ethyl acetate. A 8N aqueous sodium hydroxide solution was added to basify the aqueous layer, and the mixture was extracted with ethyl acetate. The extract was washed with a saturated aqueous sodium hydrogen carbonate solution, water and saturated brine, dried over anhydrous magnesium sulfate, and concentrated under reduced pressure. The residue was distilled under reduced pressure (98-101C/9-10 mmHg) to give the title compound as a colorless oil (yield 2.2 g, yield 28%). 1H-NMR (CDCl3) δ: 1.32 (2H, br s), 2.30 (6H, s), 3.81 (2H, s), 6.98-7.00 (2H, m), 7.16-7.18 (1H, m).
  • 3
  • [ 98-88-4 ]
  • [ 94-98-4 ]
  • [ 84359-55-7 ]
  • 4
  • [ 16450-41-2 ]
  • [ 94-98-4 ]
  • [ 100722-94-9 ]
  • 5
  • [ 110-91-8 ]
  • [ 79-04-9 ]
  • [ 94-98-4 ]
  • [ 1421-56-3 ]
  • 6
  • [ 100-52-7 ]
  • [ 68-11-1 ]
  • [ 94-98-4 ]
  • [ 132467-24-4 ]
  • 7
  • [ 123-11-5 ]
  • [ 68-11-1 ]
  • [ 94-98-4 ]
  • [ 109934-37-4 ]
  • 8
  • [ 53216-37-8 ]
  • [ 94-98-4 ]
  • [ 51623-16-6 ]
  • 10
  • [ 22980-09-2 ]
  • [ 94-98-4 ]
  • [ 80554-85-4 ]
  • 11
  • [ 22980-10-5 ]
  • [ 94-98-4 ]
  • [ 80554-82-1 ]
  • 14
  • [ 94-98-4 ]
  • ethyl 2-(naphthalene-2-yl)acetimidate hydrochloride [ No CAS ]
  • N-(2,4-Dimethyl-benzyl)-2-naphthalen-2-yl-acetamidine; hydrochloride [ No CAS ]
  • 15
  • [ 94-98-4 ]
  • [ 61554-51-6 ]
  • [ 80884-23-7 ]
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