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[ CAS No. 89226-13-1 ] {[proInfo.proName]}

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Chemical Structure| 89226-13-1
Chemical Structure| 89226-13-1
Structure of 89226-13-1 * Storage: {[proInfo.prStorage]}

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Quality Control of [ 89226-13-1 ]

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Product Details of [ 89226-13-1 ]

CAS No. :89226-13-1 MDL No. :MFCD09025922
Formula : C7H14N2O2S Boiling Point : -
Linear Structure Formula :- InChI Key :AGBIUUFZUPNDTM-UHFFFAOYSA-N
M.W : 190.26 Pubchem ID :5324304
Synonyms :
Chemical Name :tert-Butyl (2-amino-2-thioxoethyl)carbamate

Safety of [ 89226-13-1 ]

Signal Word:Warning Class:N/A
Precautionary Statements:P261-P305+P351+P338 UN#:N/A
Hazard Statements:H302-H315-H319-H335 Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 89226-13-1 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 89226-13-1 ]

[ 89226-13-1 ] Synthesis Path-Downstream   1~11

  • 1
  • [ 421-20-5 ]
  • [ 89226-13-1 ]
  • [ 140903-34-0 ]
  • 2
  • [ 90929-73-0 ]
  • [ 89226-13-1 ]
  • [ 1001412-80-1 ]
YieldReaction ConditionsOperation in experiment
81% In acetonitrile; at 20 - 80℃; for 22h; Compound 14.1 (0.308 grams, 1.28 mmol) was mixed with Compound 14.2 (0.245 grams, 1.28 ramol) and AcCN (6 ml) was added. The reaction was stirred at ambient temperature for 20 hours followed by 80 C for 2 hours. The mixture was cooled to room temperature, diluted with EtOAc, washed with saturated sodium bicarbonate, brine, dried over sodium sulfate, filtered, and concentrated to yield Compound 14.3 (0.344 grams, 1.04 mmol, 81 %). ES (+) MS m/e = 331 (M+l).
  • 3
  • [ 1001412-89-0 ]
  • [ 89226-13-1 ]
  • [ 1001412-91-4 ]
YieldReaction ConditionsOperation in experiment
19% In ethanol; for 16h;Heating / reflux; Compound 17.1 (1.0 gram, 3.95 mmol) and Compound 14.2 (0.752 grams, 3.95 mmol) were dissolved in EtOH (20 ml) and heated at reflux for 16 hours. The mixture was cooled to ambient temperature, diluted with DCM, washed with saturated sodium bicarbonate, dried over sodium sulfate, filtered, and concentrated to yield Compound 17.2 (0.254 grams, 0.737 mmol, 19%). ES (+) MS m/e = 345 (M+l).
  • 6
  • [ 4530-20-5 ]
  • Fmoc-L-Leu-F [ No CAS ]
  • [ 89226-13-1 ]
  • 10
  • [ 89226-13-1 ]
  • {N-[3-(tert-Butoxycarbonylamino-methyl)-phenyl]-carbamimidoylmethyl}-carbamic acid tert-butyl ester; hydrobromide [ No CAS ]
  • 11
  • [ 4530-20-5 ]
  • [ 89226-13-1 ]
YieldReaction ConditionsOperation in experiment
100% With Lawessons reagent; In dichloromethane; at 25℃; for 16h; Boc-glycine (2.34 g, 0.134 mmol) was dissolved in dichloromethane (130 mL) and treated with Lawesson's reagent (2.9 g, 0.52 equivalents) and the mixture was stirred at 25 C. for 16 h. The mixture was filtered and the solvents were evaporated. The residue was purified using dichloromethane:ethyl acetate (1:1) to give 2.56 g (100%) of the thioamide.
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