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[ CAS No. 89-05-4 ] {[proInfo.proName]}

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Chemical Structure| 89-05-4
Chemical Structure| 89-05-4
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Product Details of [ 89-05-4 ]

CAS No. :89-05-4 MDL No. :MFCD00002471
Formula : C10H6O8 Boiling Point : -
Linear Structure Formula :(C6H2)(C(O)OH)4 InChI Key :CYIDZMCFTVVTJO-UHFFFAOYSA-N
M.W : 254.15 Pubchem ID :6961
Synonyms :

Safety of [ 89-05-4 ]

Signal Word:Warning Class:N/A
Precautionary Statements:P261-P280-P302+P352-P305+P351+P338 UN#:N/A
Hazard Statements:H315-H319-H335 Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 89-05-4 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 89-05-4 ]

[ 89-05-4 ] Synthesis Path-Downstream   1~8

  • 1
  • [ 7343-34-2 ]
  • zinc(II) nitrate hexahydrate [ No CAS ]
  • [ 89-05-4 ]
  • [Zn2(3,5-dimethyl-1-H-1,2,4-triazole)2(1,2,4,5-benzenetetracarboxylate)(H2O)2]n [ No CAS ]
  • 2
  • [ 143131-66-2 ]
  • [ 89-05-4 ]
  • [ 6147-53-1 ]
  • 2C10H2O8(4-)*5Co(2+)*C12H12N6*2HO(1-)*4H2O [ No CAS ]
YieldReaction ConditionsOperation in experiment
38% A mixture of Co(OAc)2·4H2O (0.10 mmol, 24.9 mg),1,2,4,5-benzenetetracarboxylatic acid (0.10 mmol, 25.4 mg), <strong>[143131-66-2]1,4-bis(1,2,4-triazol-1-ylmethyl)benzene</strong> (0.10 mmol, 24.0 mg) in 10 mL of distilled H2O was stirred for20 min in air, and the pH value of the mixture was adjusted to approximately 6 by NaOH (0.10 mol/dm3), then transferred to a 25 mL Teflon-lined stainless vessel and heated to 140 C for 3 days under autogenous pressure. Purple block crystalsof the complex were obtained after the autoclave was cooled to room temperature at a rate of 5 C/h. With Co(OAc)2·4H2O. Yields: ca. 38% based on Co. Anal. Calcd.for C32H26Co5N6O22 (Fw = 1141.24): C, 33.68; H, 2.30; N, 7.36. Found: C, 33.26; H,2.59; N, 7.62. IR (KBr, cm-1) for the compelx: 3449vs, 2365 s, 1668 m, 1613 m,1544 m, 1412 m, 1086 m, 879w, 796w, 671w, 546w.
  • 3
  • [ 89-05-4 ]
  • [ 18653-98-0 ]
  • 2C16H20N2O2*C10H6O8*H2O [ No CAS ]
YieldReaction ConditionsOperation in experiment
77% In N,N-dimethyl-formamide; for 0.5h;Heating; Mixture of H4BTtC (0.25 g, 1.00 mmol) and BzE (0.27 g,1.00 mmol) were dissolved in 5 mL of DMF and heated for30 min. The resultant solution was filtered and allowed to stand at room temperature. Colorless block-shaped crystals were obtained by slow evaporation of the solution in 77 % (0.32 g, 0.77 mmol) yield. Anal Calc. for C45H55N5O14: C,60.73; H, 6.23; N, 7.87. Found: C, 60.37; H, 6.05; N,7.44 %. IR (KBr, cm-1): 3400, 3100, 2730, 2617, 1869,1673, 1608, 1570, 1457, 1396, 1274, 1249, 1178, 878, 753,721, 607, 465.
  • 4
  • [ 89-05-4 ]
  • [ 86119-84-8 ]
  • [ 7732-18-5 ]
  • [ 112881-51-3 ]
  • zinc dibromide [ No CAS ]
  • [Zn(HPO4)(4′-(4-pyridyl)-2,2′:6′,2′′-terpyridine)]2*(1,2,4,5-benzenetetracarboxylic acid)2*(H2O) [ No CAS ]
YieldReaction ConditionsOperation in experiment
60% at 140℃; for 48h;Autoclave; High pressure; ZnBr2 (45 mg, 0.2 mmol), 4?-(4-pyridyl)-2,2?:6?,2?-terpyridine (31mg, 0.1mmol), 1,2,4,5-benzenetetracarboxylic acid (127mg, 0.5mmol), ortho-phosphoric acid (461.2mg, 4.7mmol) were added to a solution of H2O (10mL). The slurry was then transferred into a 23mL Teflon-lined autoclave and heated at 140C for 48h. The solution was allowed to cool at a rate of 5C/h to room temperature. block-shaped crystals were collected through filtration, washed with H2O (3×20mL) and EtOH (3×20mL), dried at room temperature in a vacuum (44mg, 60% yield based on PYTPY). IR (KBr): nu=3745 (vw), 3089 (w), 1699 (vs), 1558 (vs), 1479 (m), 1418 (m), 1340 (vs), 1242 (vw), 1166 (m), 1059 (vs), 981 (vs), 794 (vs), 756 (vs), 698 (m), 597 (vs), cm-1. C60H44N8O25P2Zn2 (M=1469.71): calcd. C 48.99%, H 2.99%, N 7.62%; found C 47.56%, H 2.48%, N 7.18%.
  • 5
  • [ 89-05-4 ]
  • [ 3347-62-4 ]
  • C10H6O8*2C10H10N2 [ No CAS ]
YieldReaction ConditionsOperation in experiment
63% In methanol; for 0.25h;Heating; General procedure: A methanolic (10 mL) solution of H4BTtC (0.25 g, 1.00 mmol) and PzH (0.07 g, 1.00 mmol) was heated for 15 min. The resultant colorless solution was filtered and allowed to stand at room temperature. Colorless block shape crystals obtained by slow evaporation of the solvent.
  • 6
  • [ 4054-67-5 ]
  • [ 89-05-4 ]
  • C10H6O8*C10H14N4 [ No CAS ]
YieldReaction ConditionsOperation in experiment
74% In methanol; for 0.25h;Heating; General procedure: A methanolic (10 mL) solution of H4BTtC (0.25 g, 1.00 mmol) and PzH (0.07 g, 1.00 mmol) was heated for 15 min. The resultant colorless solution was filtered and allowed to stand at room temperature. Colorless block shape crystals obtained by slow evaporation of the solvent.
  • 7
  • [ 4054-67-5 ]
  • [ 89-05-4 ]
  • ammonium iron (II) sulfate [ No CAS ]
  • [ 68-12-2 ]
  • [NH4][Fe2(OH)(BTtC)(3,3',5,5'-tetramethyl-4,4'-bipyrazole)0.5(H2O)(DMF)]*DMF*3H2O [ No CAS ]
  • 8
  • cobalt(II) nitrate hexahydrate [ No CAS ]
  • [ 89-05-4 ]
  • [ 69506-85-0 ]
  • [Co2(μ-η1:η1-O2)(1,3-bis(imidazol)propane)2(benzene-1,2,4,5-tetracarboxylate)]n [ No CAS ]
YieldReaction ConditionsOperation in experiment
72% In water; at 130℃; for 72h;Autoclave; High pressure; General procedure: A solution of 4,4′-oxybis(benzoate) (0.10 mmol, 25.8 mg),1,3-bis(imidazol)propane (0.10 mmol, 17.6 mg) andCo(NO3)2·6H2O (0.10 mmol, 29.1 mg) in distilled water(15 mL) was placed in a Teflon-lined stainless steel vessel,heated to 130 C for 3 days and then cooled to roomtemperature over 24 h. The resulting solid was washed with methanol and dried under vacuum.
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