Purity | Size | Price | VIP Price | USA Stock *0-1 Day | Global Stock *5-7 Days | Quantity | ||||||
{[ item.p_purity ]} | {[ item.pr_size ]} | Inquiry |
{[ getRatePrice(item.pr_usd, 1,1,item.pr_is_large_size_no_price) ]} {[ getRatePrice(item.pr_usd,item.pr_rate,1,item.pr_is_large_size_no_price) ]} |
{[ getRatePrice(item.pr_usd, 1,1,item.pr_is_large_size_no_price) ]} | Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price) ]} {[ getRatePrice(item.pr_usd,1,item.mem_rate,item.pr_is_large_size_no_price) ]} | {[ item.pr_usastock ]} | in stock Inquiry - | {[ item.pr_chinastock ]} | {[ item.pr_remark ]} in stock Inquiry - | Login | Inquiry |
Please Login or Create an Account to: See VIP prices and availability
CAS No. : | 886365-02-2 | MDL No. : | MFCD07375100 |
Formula : | C7H6BrNO2 | Boiling Point : | No data available |
Linear Structure Formula : | - | InChI Key : | RMSVDYVOLGRLNJ-UHFFFAOYSA-N |
M.W : | 216.03 | Pubchem ID : | 45790031 |
Synonyms : |
|
Signal Word: | Warning | Class: | |
Precautionary Statements: | P261-P280-P305+P351+P338 | UN#: | |
Hazard Statements: | H302-H315-H319-H332-H335 | Packing Group: | |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
With triethylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; | Compound 7-105 was synthesized as follows: 2-(4-(4-methoxybenzoyl)piperidinylcarbonyl)-4-methyl-5-bromopyridine: To a mixture of 5-bromo-4-methylpyridine-2-carboxylic acid (0.400 g, 1.85 mmol, 1.0 eq) and <strong>[25519-82-8]4-(4-methoxybenzoyl)piperidine hydrochloride</strong> (0.474 g, 1.85 mmol, 1.0 eq) was added dimethylformamide (10 mL) followed by triethylamine (0.64 mL, 4.36 mmol, 2.5 eq). HATU (0.774 g, 2.04 mmol, 1.1 eq) was added forming a yellow solution, which was stirred at room temperature for 1 day. The reaction was partitioned between EtOAc (120 mL) and water-NaHCO3 (1:1, 120 mL). The organics were further washed with brine (120 mL), water (120 mL) and brine (100 mL), dried (Na2SO4) and concentrated under reduced pressure. MPLC (0?10% MeOH-CH2Cl2) yielded the title compound (0.693 g, 89%) as a yellow oil; 1H nmr (CDCl3) delta 8.55 (1H, s, pyH-3 or H-6), 7.90 (2H, d, J 9.0 Hz, 2H of C6H4OMe), 7.48 (1H, s, pyH-3 or H-6), 6.91 (2H, d, J 9.0 Hz, 2H of C6H4OMe), 4.64 (1H, m, 1H of BzpipH-2, H-6), 4.01 (1H, m, 1H of BzpipH-2, H-6), 3.83 (3H, s, OCH3), 3.49 (1H, m, BzpipH-4), 3.23 (1H, m, 1H of BzpipH-2, H-6), 3.03 (1H, m, 1H of BzpipH-2, H-6), 2.39 (3H, s, pyCH3), 1.95 (1H, m, 1H of BzpipH-3, H-5), 1.86-1.75 (3H, s, 3H of BzpipH-3, H-5); m/z 417, 419 [M+H]+. |
[ 886365-06-6 ]
Methyl 5-bromo-4-methylpicolinate
Similarity: 0.91
[ 886365-43-1 ]
5-Bromo-3-methylpicolinic acid
Similarity: 0.86
[ 886364-94-9 ]
5-Bromo-4-methylpicolinaldehyde
Similarity: 0.85
[ 1394291-59-8 ]
(5-Bromo-4-methylpyridin-2-yl)methanol
Similarity: 0.85
[ 886365-43-1 ]
5-Bromo-3-methylpicolinic acid
Similarity: 0.86
[ 1196154-93-4 ]
4-Bromo-5-methylpicolinic acid
Similarity: 0.85
[ 870997-85-6 ]
3-Amino-5-bromopyridine-2-carboxylic Acid
Similarity: 0.81
[ 886365-06-6 ]
Methyl 5-bromo-4-methylpicolinate
Similarity: 0.91
[ 886365-43-1 ]
5-Bromo-3-methylpicolinic acid
Similarity: 0.86
[ 886364-94-9 ]
5-Bromo-4-methylpicolinaldehyde
Similarity: 0.85
[ 1394291-59-8 ]
(5-Bromo-4-methylpyridin-2-yl)methanol
Similarity: 0.85