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[ CAS No. 885521-88-0 ] {[proInfo.proName]}

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Chemical Structure| 885521-88-0
Chemical Structure| 885521-88-0
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Product Details of [ 885521-88-0 ]

CAS No. :885521-88-0 MDL No. :MFCD07781599
Formula : C7H4BrIN2 Boiling Point : No data available
Linear Structure Formula :- InChI Key :POXUFQBYDQCUFO-UHFFFAOYSA-N
M.W : 322.93 Pubchem ID :24728212
Synonyms :

Safety of [ 885521-88-0 ]

Signal Word:Warning Class:
Precautionary Statements:P261-P305+P351+P338 UN#:
Hazard Statements:H302-H315-H319-H335 Packing Group:
GHS Pictogram:

Application In Synthesis of [ 885521-88-0 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 885521-88-0 ]

[ 885521-88-0 ] Synthesis Path-Downstream   1~3

  • 1
  • [ 885521-88-0 ]
  • [ 1151802-22-0 ]
  • 6-bromo-3-(1-cyclopropyl-1H-pyrazol-4-yl)-1H-indazole [ No CAS ]
YieldReaction ConditionsOperation in experiment
64% To a resealable vial was added 77 K2CO3 (1.71g, 12.4mmol), 182 6-bromo-3-iodo-1H-indazole (2g, 6.2mmol), 41-183 <strong>[1151802-22-0]cyclopropyl-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1H-pyrazole</strong>(1.45g, 6.2mmol). The vial was sealed and evacuated and purged with Ar for 5min before addition of PdCl2(dppf)-CH2Cl2 Adduct (253mg, 0.310mmol), dissolved in 79 1,4-dioxane/80 water (10mL, 4:1, v/v) was then added to this solution before the vial was heated to 80C overnight. The reaction was cooled to room temperature, which was then brought to basic using 81 aqueous sodium bicarbonate solution and extracted with ethyl acetate. The resulting mixture was concentrated to give the crude product, which was purified by silica gel column chromatography. The resulting mixture was concentrated to give the crude 184 product, which was purified by silica gel column chromatography. Pale yellow solid(1.2g, 64%). 1H NMR (400MHz, Chloroform-d) delta 8.04 (s, 1H), 7.99 (s, 1H), 7.70 (d, J=8.6Hz, 1H), 7.52 (d, J=1.5Hz, 1H), 7.27 (dd, J=8.8, 1.4Hz, 1H), 3.71 (tt, J=7.4, 3.8Hz, 1H), 1.25-1.18 (m, 2H), 1.13-1.03 (m, 2H). LRMS m/z: 303 ([M+H] +).
  • 2
  • [ 885521-88-0 ]
  • [ 568577-88-8 ]
  • 4-methyl-3-(3-(4-morpholinophenyl)-1H-indazol-6-yl)-N-(3-(trifluoromethyl)phenyl)benzamide [ No CAS ]
  • 3
  • [ 885521-88-0 ]
  • [ 568577-88-8 ]
  • C17H16BrN3O [ No CAS ]
YieldReaction ConditionsOperation in experiment
General procedure: To a resealable vial was added 77 K2CO3 (1.71g, 12.4mmol), 182 6-bromo-3-iodo-1H-indazole (2g, 6.2mmol), 41-183 cyclopropyl-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1H-pyrazole(1.45g, 6.2mmol). The vial was sealed and evacuated and purged with Ar for 5min before addition of PdCl2(dppf)-CH2Cl2 Adduct (253mg, 0.310mmol), dissolved in 79 1,4-dioxane/80 water (10mL, 4:1, v/v) was then added to this solution before the vial was heated to 80C overnight. The reaction was cooled to room temperature, which was then brought to basic using 81 aqueous sodium bicarbonate solution and extracted with ethyl acetate. The resulting mixture was concentrated to give the crude product, which was purified by silica gel column chromatography. The resulting mixture was concentrated to give the crude 184 product, which was purified by silica gel column chromatography.
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